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Curriculum | Inorganic Special -V (Code-09040402) | Fourth Sem | Master of Chemistry

Curriculum

Inorganic Special -V  (Code-09040402)

S.N/Unit Topic Learning Objectives Teaching Guidelines Methodology Time                         (Hours)
1 Study of electrons at and across interfaces; electrochemical and chemical reactions Basic principles To cover basic principles; Residual current, migration current, diffusion current and limiting current; Saturated calomel electrode(SCE) and dropping mercury electrode(DME);Use of Ilkovic equation and  Koutecky equation for diffusion current;  Polarographic waves(anodic and cathodic) and Half wave potentials; Oxygen interference and maxima ; Function of supporting electrolyte Conventional 15
Residual current, migration current, diffusion current and limiting current Conventional
Saturated calomel electrode(SCE) and dropping mercury electrode(DME) Presentation
Use of Ilkovic equation and  Koutecky equation for diffusion current Conventional
Polarographic waves(anodic and cathodic) and Half wave potentials Conventional
Oxygen interference and maxima Conventional
Function of supporting electrolyte Conventional
2 Study of determination of stability constants of complexes (reversible systems only) by D.C.Polarography Catalytic hydrogen wave. To cover Catalytic hydrogen wave;  Principles of amperometric titrations, types of titration curves, and apparatus and techniques; Hanging mercury drop electrode and rotating droping mercury electrode; Platinum electrodes(RPE), Gold electrode;Carbon paste electrode, glassy carbon electrode and graphite electrode Conventional 15
Principles of amperometric titrations, types of titration curves, and apparatus and techniques. Conventional
Hanging mercury drop electrode and rotating droping mercury electrode Conventional
Platinum electrodes(RPE), Gold electrode Conventional
Carbon paste electrode, glassy carbon electrode and graphite electrode. Conventional
3 Study of Super imposed A.C. Polarography Voltametry in quiet and stirred solution with electrode other than Mercury To cover Voltametry in quiet and stirred solution with electrode other than Mercury;  Square-wave polarography, normal and differential pulse polarography; chronopotentiometry; chronoamperometry; coulometry Conventional 15
Square-wave polarography, normal and differential pulse polarography Conventional
Chronopotentiometry Conventional
Chronoamperometry Conventional
Coulometry Conventional
4 Study of theory of anodic stripping voltametry Concentration process, rest period, and stripping process To cover Concentration process, rest period, and stripping process; Cathodic stripping voltametry, Anodic deposition, and  Cathodic redissolution; Experiments and applications of above system to Inorganic systems; Theory of ion selective electrodes (ISE);  Demonstrate experiments and applications of ISE to Inorganic systems Conventional 15
Cathodic stripping voltametry, Anodic deposition, and  Cathodic redissolution Conventional
Experiments and applications of above system to Inorganic systems. Conventional
Theory of ion selective electrodes (ISE) Conventional
Demonstrate experiments and applications of ISE to Inorganic systems Presentation