Techniques in Chemistry
Paper Code: 09040208
S.No. | Topic | Domain | Time |
1 | Atomic Absorption Spectroscopy –
1.Principles, 2.Instrumentation, Sensitivity and detection limits, 3. Interferences in AAS and their elimination. |
Must Know |
5 |
2. | Atomic Emission Spectroscopy-
1. Principles 2. Sources for excitation, 3. Instrumentation, 4. Qualitative and quantitative Analysis.
|
Must Know |
8 |
3. | Flame Photometry-
1. Principles, 2. Interferences, Evaluation methods in Flame Photometry, 3. Principle and Applications of TGA and DTA. . |
Must Know |
8 |
3. | Nanomaterials Technology:
1. Nanomaterials and their historical perspective. 2. Applications of nanoscience and nanotechnology in various fields. 3. Unique properties of nanomaterials due to their nanosize, Quantum dots, 4. Techniques for their synthesis:- Hydrothermal, Solvothermal, Microwave irradiation, sol-gel, Precipitation, Reverse Micelle Synthesis, Physical Vapour deposition (PVD), Chemical Vapour Deposition (CVD), Electro deposition, 5. Characterization of nanomaterials by X-ray diffraction (XRD), Scanning Electron Microscope (SEM), Energy dispersive X-ray Analysis. Transmission Electron Microscope (TEM), Atomic Force microscopy (AFM) techniques. 6. Properties of nanostructured materials: opticals, magnetic, chemical and photo catalytic properties.
|
Desirable to know
Must Know |
10 |
4. | Purification of organic compounds using
1.chromatographic techniques: 2. paper chromatography, 3. Thin- Layer Chromatography, 4. Column Chromatography, 5. High Pressure Liquid Chromatography (HPLC), 6. Gas Chromatography, 7. Ion-Exchange Chromatography, 8. Counter- Current distribution and Electrophoresis
|
Must Know |
8 |
Book Recommended
- Poole, Charles P., Jr. Frank and J. Owens. Introduction to Nanotechnology. Wiley India
- Sachdeva, Mamta. V. Basics of Nanochemistry.
- Sergeev, G. B. and K. L. Klabunde.Nanochemistry. 2013. Elsevier.
- Fahrner, W.R. Nano Technology and Nanoelectronics. Springer International.
- Vantra, M. D., S. Evoy and J.R. Heflin-Introducation to Nanoscience and Technology.
- Edited Springer.
- Lindsey, S. M. Introduction to Nanosciences. Oxford Press.
- Muralidharan, V. S. and A. Subramania. Nano Science and Technolony.
- Budhiraja, R.P. Basic Concepts of Analytical Chemistry by S.M. Khopkar,
- New age International Publishers.
- Sharma,B.K. Instrumental Methods of Chemical Analysis. Goel Publishing House.